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A gradient LC elution program was utilized for mobile phases consisting of 0.1% formic acid (0.1% v/v) in ultrapure water (buffer A), and acetonitrile plus 0.1% (v/v) formic acid (buffer B) at a flow rate of 0.4 mL/min
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10.1016/j.jaad.2010.11.061 12 AlkhateebA.FainP
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